SYLLABUS
Unit-1: Titrimetric Analysis
1 Non-Aqueous Titrations
1.1 Introduction
1.2 Theory and Principle
1.3 Solvents
1.4 Indicators
1.5 Types of Non-aqueous Titrations
1.6 Methods for Determining End Point
1.7 Applications
2 Oxidation-Reduction Titrations
2.1 Introduction
2.2 Types of Redox Titrations
2.2.1 Permanganometric Titrations/Permanganometry
2.2.2 Titrations Involving Iodine
2.2.3 Titrations Involving Ammonium
Cerium (IV) Sulphate/Ceriometry
2.3 Indicators Used in Redox Titrations
3 Complexometric Titrations
3.1 Introduction
3.2 Theory
3.3 Types of Complexometric Titrations
3.4 Methods for Detecting End Point
3.5 Stability of Complex Compounds
3.6 Masking and Demasking Agents
3.7 Applications of Complexometric Titrations
4 Diazotization Methods
4.1 Introduction
4.2 Principle and Theory
4.3 Applications
Unit-2: Quantitative Analysis of Functional Groups
1 Introduction
2 Determination of Amines
2.1 Acylation of Primary and Secondary Amines
2.2 Diazotization of Primary Aromatic Amines
2.3 Other Methods
3 Determination of Esters
3.1 Saponification
3.2 Procedure Using Ion-Exchange Resins
3.3 Specific Methods
3.4 Spectroscopic Methods
3.5 Other Methods
4 Determination of Carbonyl Compounds
4.1 Methods Based on Condensation Reactions
4.2 Other Methods
5 Determination of Hydroxyl and Carboxyl Groups
5.1 Determination of Hydroxyl Group
5.2 Determination of Carboxyl Group
5.2.1 Titrimetric Determination of Acids
5.2.2 Spectrophotometric Methods
5.2.3 Chromatographic Methods
5.2.4 Other Methods
Unit-3: Analytical Reagents
1 Introduction
2 MBTH Reagent
3 FC Reagent
4 PDAB Reagent
5 2,3,5-Triphenyltetrazolium Salt
6 2,6-Dichloroquinone Chlorimide.
7 BM Reagent
Unit-4: AAS and Radiochemical Methods of Analysis
1 Atomic Absorption
Spectrometry (AAS)
1.1 Introduction
1.2 Principle
1.3 Instrumentation
1.4 Interferences
1.5 Elemental Analysis
1.6 Applications
2 Radiochemical methods
2.1 Introduction
2.2 Types of Radiations
2.3 Radioactive Decay and Units of Radioactivity
2.4 Measurement of Radioactivity
2.5 Tagging of Compounds
2.6 Labelled Reagents
2.7 Isotope Dilution Method
2.8 Radioimmunoassay (RIA)
Unit-5: Dissolution Method Development, Microbiological
Assays and Biological Tests
1 Dissolution Method Development
and Validation
1.1 Introduction
1.2 Preliminary Assessment
1.3 Dissolution Method Development
1.4 Automated Systems.
1.5 Validation of Dissolution Procedure
2 Microbiological Assays and
Biological Testing
2.1 Antimicrobial Effectiveness Testing (AET)
2.2 Microbial Limit Tests
2.3 Sterility Tests.
2.4 Microbial Assay of Antibiotics
2.5 Bacterial Endotoxin Tests
unit-wise Previously Asked questions & important questions P.1 – P.4
